Non-innocence of β-diketiminato ligands

Gondzik, Sebastian GND; Bläser, Dieter; Wölper, Christoph GND; Schulz, Stephan GND

The homoleptic thio-β-ketiminate zinc complex [MesNC(Me)CH{C(Me)NMes}S]2Zn (1) was obtained from reactions of elemental sulfur with the β-diketiminato zinc complexes [CH{C(Me)NMes}2]ZnMe, [CH{C(Me)NMes}2]2Zn2 and [[CH{C(Me)NMes}2]Zn-TePh]2. 1 and the byproducts were characterized by multinuclear NMR (1H, 13C, 125Te) and IR spectroscopy, elemental analyses as well as by single crystal X-ray diffraction.

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Gondzik, S., Bläser, D., Wölper, C., Schulz, S., 2020. Non-innocence of β-diketiminato ligands. https://doi.org/10.1016/j.jorganchem.2015.02.028
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