Synthesis and X-ray crystal structures of homotrimetallic Zinc Bisureate Complexes

Bayram, Melike GND; Schulz, Stephan GND; Wölper, Christoph GND

Alkane elimination reactions of the tethered bis(urea) proligand 1,4‐(tBuNHCONH)2‐C4H8 (1) with ZnR2 (R = Me, Et, nPr) yielded trimetallic zinc complexes [RZn‐1,4‐(tBuNHCON)2‐C4H8]2Zn [R = Me (2), Et (3), and nPr (4)]. 2 4 were characterized by heteronuclear NMR (1H, 13C) and IR spectroscopy, elemental analysis, and single‐crystal X‐ray diffraction.

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Bayram, M., Schulz, S., Wölper, C., 2020. Synthesis and X-ray crystal structures of homotrimetallic Zinc Bisureate Complexes. https://doi.org/10.1002/zaac.201700350
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