Structural characterization of Sb2Et4 and Bi2Et4

Kuczkowski, Andreas GND; Heimann, Stefan GND; Weber, Anna; Schulz, Stephan GND; Bläser, Dieter; Wölper, Christoph GND

The solid state structures of Et4Sb2 1 and Et4Bi2 2 were determined by single crystal Xray diffraction. Single crystals of 1 and 2 were grown in a closed quartz glass capillary under an inert argon atmosphere on the diffractometer using a specific IR-laser-assisted technique. 1 shows short intermolecular Sb···Sb interactions, whereas the closest Bi···Bi distances are longer than the sum of the van-der-Waals radii.

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Kuczkowski, A., Heimann, S., Weber, A., Schulz, S., Bläser, D., Wölper, C., 2020. Structural characterization of Sb2Et4 and Bi2Et4. https://doi.org/10.1021/om2005723
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