Lewis acid-base adduct Me3Sb-Ga(t-Bu)3

Schulz, Stephan GND; Kuczkowski, Andreas GND; Nieger, Martin ORCID

The simple Lewis acid–base adduct Me3Sb–Ga(t-Bu)31 was prepared by reaction of t-Bu3Ga and SbMe3 in 1:1 M ratio. 1 was fully characterized by multinuclear NMR spectroscopy (1H, 13C). In addition, its solid state structure was determined by single crystal X-ray diffraction studies. 1 is monoclinic, space group P21/n with a = 8.4895(2) Å, b = 12.9303(4) Å, c = 17.9976(5) Å, β = 97.472(2)° and Z = 4.

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Schulz, S., Kuczkowski, A., Nieger, M., 2020. Lewis acid-base adduct Me3Sb-Ga(t-Bu)3. https://doi.org/10.1007/s10870-010-9815-6
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